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For the
examination of liquids open the prism box and place a few drops
upon the ground surface of the lower prism. Close and fasten the
prism box when the liquid will be squeezed into a thin film
between the prism. Focus the crosswire with the eyepiece, adjust
the mirror until the illumination is good, and gently turn the
prism box by means of a milled head screw forwards and backwards
until a coloured band appears in he field of view. By turning
the milled ring at the base of the telescope, a position will be
found at which the coloured band will be eliminated, the field
of view being partly light and partly dark with a sharp dividing
line. Bring this sharp dividing line into coincidence with the
intersection of the crosswires and read the refractive index or
sugar percentage on the divided arc by means of the magnifier.
The scale is
divided to the third decimal place, the fourth being easily
oriented by estimation. It will be noted that the hing of the
prism box is so constructed that the lower prism in the box may
be removed. For the examination of plastic bodies such as resin,
remove the lower prism box, soften the material by heat, and
smear a little on the exposed surface of the upper prism, then
proced as above. To examine crystals or glasses. A specimen
should be prepared, similar in shape to the standard glass test
piece provided. Moisten the polished surface of the specimen
with the smallest possible quantity of monobromonapthalene and
place it upon the suface of the prism with the ground edge
directed towards the mirror. Care must be taken to avoid excess
of monobromonathalne as this may spoil the definition and
confuse the reading. When the correct quantity is used, the
specimen will adhere firmly to the prism face.The instrument is
sent out carefully adjusted, but it is as well to verify the
setting by applying the class test piece to the prism and
nothing if the reading is that marked on the piece. I this is
not the case, adjust the small squared screw at the back of the
telescope with the key provided until agreement is secured. The
mean of several reading should be taken if great accuracy is
desired. |
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An ideal
instrument for quality control with better accuracy. Suitable
for testing sugar solution and other optically active liquids.
Accommodate 220 mm. length tube. The polarimeter consists
basically of two polarizing elements of 'Polaroid' one of which
is fixed, the other capable of rotation and mounted within a
graduated scale in order to measure its orientation with respect
to the other. When the planes of polarisation of the two
elements are mutually perpendicular no light is transmitted
through the system. A thin plate of quartz is positioned to
cover half the aperture of one of the elements in order to
introduce a 'half shadow effect'. The effects to cause an
extinction of light in one half of the field a few degrees
normally 7 degrees, before the other half of the field reaches
its extinction position. Thus a balance can be achieved where
one half of the field is reducing in intensity as the other half
is increasing, as the scale is rotated. The position of the
scale at which the two halves are of equal intensity is the
balance position and is used in all determinations. On
introducing an optically active sample between the polarizing
elements the balance is disturbed and it is necessary to
rebalance by turning the scale. The amount by which the scale is
moved a direct measure of the sample optical activity. |
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An ideal
instrument for quality control with better accuracy. Suitable
for tesing sugar solution and oher optically active liquids.
Accomodate 400 mm. length tube.The polarimeter consists
basically of two polarising elements of 'Polaroid' one of which
is fixed, the other capable of rotation and mounted within a
graduated scale in order to measure its orientation with respect
to the other. When the planes of polarisation of the two
elements are mutually perpendicular no light is transmitted
through the system. A thin plate of quartz is positioned to
cover half the aperture of one of the elements in oder to
introduce a 'half shadow effect'. The effectis to cause an
extinction of light in one half of the field a few degrees
normally 7 degrees, before the other half of the field reaches
its extinction position. Thus a balance can be achieved where
one half of the field is reducing in intensity as the other half
is increasing, as the scale is rotated. The position of the
scale at which the two halves are of equal intensity is the
balance position and is used in all determinations. On
introducing an optically active sample between the polarising
elements the balance is disturbed and it is necesary to
rebalance by turning the scale. The amount by which the scale is
moved a direct measure of the sample optical activity. |